
All electrochemical data was collected between 24/05/2024 - 14/04/2026

Electrochemical data used to create the averaged plots within the paper are given in this folder. The duplicate cells for the asymmetric cycling for the recovered TNO at 160C are in the Electrochemistry file.

Mass of active material for each cell:

Recovered TNO 160C
Cell 1_Cu_PVDF: 1.25 mg	Cell 3_Cu_PVDF: 1.54 mg		

Recovered TNO 140C
RTNO(5)_Rate_Test_Cu_PVDF: 1.00 mg	

Benchmark Cell
Benchmark_Cell_Cu_PVDF: 5.42 mg	

Pristine Cell
TNO(3)_cal_Cu_PVDF: 6.66 mg


The rate studies for these materials were performed asymmetrically such that on lithiation a current density of 0.1 A g-1 was consistently applied with the constant voltage step (with 20% current decay limit). The delithiation rate was gradually increased from 0.1 to 4 A g-1 with 5 cycles at each step. Asymmetric cycling was introduced to reduce the current rate limitations created by the use of Li metal in an organic electrolyte. After the rate study, five further cycles were conducted at 0.1 A g-1.



