Experiment FL 1a,91.71°C at t = 0,,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,Experiment FL 15a,90.06°C at t = 0,min = 87.11°C,Ret time 5.113,PLA grade 2500HP,,NMR,NMR,NMR,,,,,,,,,Experiment FL 30a,89.86°C at t = 0,min = 87.6°C,Ret time 5.091,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
0,91.71,1,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,0,90.06,1.8,0,0,0,100,0,0,,,,,,,,,0,89.86,2.3,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
5,89.74,0.9,0.8,0,5,100,0,0,,,,,,,,,,,,,,,,,,10,91.7,1.7,7.51,0.002,10,83,16,1,,,,,,,,,10,91.04,2.3,37.3,0.001,10,77,22,1,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
10,91.71,1,1.89,0.0005,10,85,13,2,,,,,,,,,,,,,,,,,,20,90.35,1.8,24.29,0.004,20,69,27,4,,,,,,,,,30,90.11,2.1,94.44,0.003,30,66,32,2,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
15,92.67,2,11.3,0.002,15,77,21,2,,,,,,,,,,,,,,,,,,40,90.04,1.9,56.01,0.01,40,46,41,13,,,,,,,,,60,90.01,2,121.95,0.005,60,58,37,5,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
25,89.89,1,17.41,0.003,25,64,28,8,,,,,,,,,,,,,,,,,,60,90.01,1.8,82.61,0.015,60,35,46,19,,,,,,,,,120,90.01,1.9,197.47,0.009,120,49,43,8,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
40,90.03,1.1,52.81,0.009,40,52,38,10,,,,,,,,,,,,,,,,,,90,89.95,1.9,126.96,0.023,90,23,46,31,,,,,,,,,180,90,1.8,257.03,0.012,180,42,46,12,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
60,90,1,75.08,0.014,60,44,43,14,,,,,,,,,,,,,,,,,,120,90,1.8,169.41,0.031,120,13,45,42,,,,,,,,,240,90,1.8,317.71,0.015,240,38,47,15,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
90,90,1.1,124.49,0.023,90,27,51,23,,,,,,,,,,,,,,,,,,150,90,1.7,211.2,0.038,150,10,39,51,,,,,,,,,900,90,1.7,885.96,0.038,900,11,48,41,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
120,89.8,1.1,175.61,0.031,120,16,46,38,,,,,,,,,,,,,,,,,,180,89.99,1.6,243.5,0.044,180,6,36,58,,,,,,,,,1398,90.01,1.7,1155.29,0.05,1398,5,41,54,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
150,90,1.1,226.38,0.04,150,12,43,46,,,,,,,,,,,,,,,,,,240,90.01,1.8,292.33,0.053,240,0,30,70,,,,,,,,,2400,90.01,1.7,1499.86,0.064,2400,2,28,70,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
180,89.99,1.1,235.38,0.043,180,9,41,50,,,,,,,,,,,,,,,,,,300,90,1.7,324.97,0.059,300,0,21,79,,,,,,,,,3090,90,1.7,1651.3,0.072,3090,0,24,76,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
240,90.01,1.1,304.04,0.055,240,7,27,66,,,,,,,,,,,,,,,,,,360,90,1.7,349.81,0.063,360,0,18,82,,,,,,,,,3870,90,1.6,1737.76,0.075,3870,0,17,83,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
300,90.01,1.1,343.36,0.062,300,0,27,73,,,,,,,,,,,,,,,,,,420,90,1.7,367.7,0.066,420,0,8,92,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
360,90,1.1,367.87,0.066,360,0,23,77,,,,,,,,,,,,,,,,,,480,90,1.8,383.82,0.069,480,0,8,92,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,540,90,1.8,389.7,0.071,540,0,7,93,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
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Experiment FL 2a,70.32°C at t = 0,,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,Experiment FL 14b,70.05°C at t = 0,min = 68°C,Ret time 5.113,PLA grade 2500HP,,NMR,NMR,NMR,,,,,,,,,Experiment FL 31b,70.15°C at t = 0,min = 68.13°C,Ret time 5.091,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
0,70.32,1,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,0,70.05,1,0,0,0,100,0,0,,,,,,,,,0,70.15,1.5,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
5,70.34,0.8,0,0,5,97,3,0,,,,,,,,,,,,,,,,,,20,70.07,1.1,6.48,0.002,20,77,20,2,,,,,,,,,10,70.93,0.8,18.8,0.001,10,60,39,1,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
10,71.43,0.9,0,0,10,92,8,0,,,,,,,,,,,,,,,,,,40,69.99,1,12.67,0.003,40,73,24,3,,,,,,,,,30,70,0.7,92.46,0.003,30,53,40,8,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
15,70.51,1,0,0,15,89,11,0,,,,,,,,,,,,,,,,,,60,70.01,1,20.31,0.004,60,68,28,4,,,,,,,,,60,70,0.8,131.15,0.005,60,49,42,9,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
20,70.2,1,3.47,0.001,20,85,14,1,,,,,,,,,,,,,,,,,,120,70,1,45.45,0.008,120,52,38,9,,,,,,,,,120,70,0.7,177.16,0.008,120,45,44,11,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
40,70.02,1,11.26,0.002,40,79,20,1,,,,,,,,,,,,,,,,,,180,70,1,71.61,0.013,180,41,44,15,,,,,,,,,240,70,0.8,306.67,0.014,240,38,48,14,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
60,70.01,1,20.15,0.003,60,67,29,4,,,,,,,,,,,,,,,,,,240,70,1,98.57,0.018,240,31,48,21,,,,,,,,,468,70,0.7,386.12,0.017,468,35,49,16,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
90,70,1,35.1,0.007,90,60,34,6,,,,,,,,,,,,,,,,,,300,70,1,125.85,0.023,300,24,49,28,,,,,,,,,1170,70,0.7,587.58,0.026,1170,21,51,28,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
120,70,1,50.17,0.01,120,49,40,11,,,,,,,,,,,,,,,,,,420,70,1,175.93,0.032,420,15,47,38,,,,,,,,,2640,70,0.7,919.39,0.04,2640,8,48,44,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
150,69.98,1,66.61,0.012,150,42,45,13,,,,,,,,,,,,,,,,,,600,70,1,237.95,0.043,600,9,41,50,,,,,,,,,4182,70,0.7,1190,0.051,4182,2,41,47,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
180,70,1,81.98,0.015,180,38,45,17,,,,,,,,,,,,,,,,,,840,70.01,1,302.68,0.055,840,5,31,65,,,,,,,,,5904,70,0.7,1449,0.063,5904,0,34,66,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
240,70,1,109.72,0.02,240,32,46,22,,,,,,,,,,,,,,,,,,1140,70.01,1,349.34,0.063,1140,2,22,76,,,,,,,,,7224,70,0.7,1549,0.067,7224,0,27,73,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
300,70,1,145.55,0.026,300,26,47,27,,,,,,,,,,,,,,,,,,1500,70,0.9,382.5,0.069,1500,0,16,84,,,,,,,,,8478,70,0.7,1638.68,0.071,8478,0,22,78,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
360,70,1,172.34,0.033,360,16,48,36,,,,,,,,,,,,,,,,,,1920,70,0.9,407.77,0.074,1920,0,9,91,,,,,,,,,8700,70,0.7,1597.8,0.069,8700,0,21,79,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
420,70,1,203.58,0.037,420,15,45,40,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
1680,70,1.8,404.26,0.073,1680,0,9,91,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
1860,70,1.3,430.75,0.078,1860,0,5,95,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
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,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,(300 min NMR broke),,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
Experiment FL 3a,110.02°C at t = 0,min = 109.02°C,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,Experiment FL 16a,110.07°C at t = 0,min = 109.7°C,Ret time 5.113,PLA grade 2500HP,,NMR,NMR,NMR,,,,,,,,,Experiment FL 29a,110°C at t = 0,min = 109.23°C,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,Experiment FL 29b,110.04°C at t = 0,min = 107.35°C,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,Experiment FL 29c,110.05°C at t = 0,min = 107.42°C,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,Experiment FL 3b,112°C at t = 0,min = 109.21°C,Ret time 5.00,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,,
0,110.02,3,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,0,110.07,3,0,0,0,100,0,0,,,,,,,,,5,113.39,3,1.96,0,,,,,,0,110.04,3.3,0,0,,,,,,0,110.05,3.7,0,0,0,100,0,0,,,,,,,,0,,4.2,0,0,,,,,,,,,,,,,,,,,,,,,,,
5,112.98,2.9,0,0,5,90,9,1,,,,,,,,,,,,,,,,,,5,110.02,3.1,1.33,0.001,5,92,7,1,,,,,,,,,10,112.6,2.9,6.1,0,,,,,,10,111.33,3.4,3.99,0,,,,,,10,111.25,3.7,9.89,0.001,10,88,12,0,,,,,,,,10,110.85,4.2,44.44,0.001760558,,,,,,,,,,,,,,,,,,,,,,,
10,114.1,2.8,21,0.001,10,56,37,7,,,,,,,,,,,,,,,,,,10,111.74,3,16.28,0.003,10,70,27,3,,,,,,,,,20,110.08,2.7,12.58,0,,,,,,20,110.72,3.2,17.06,0.001,,,,,,30,110.14,3,59.91,0.002,30,69,29,2,,,,,,,,15,110,4,91.54,0.003626496,,,,,,,,,,,,,,,,,,,,,,,
15,111.74,2.6,40.56,0.007,15,50,40,10,,,,,,,,,,,,,,,,,,15,110.73,2.9,30.62,0.006,15,63,32,5,,,,,,,,,40,110,3,61.26,0.002,,,,,,30,110.15,3.1,31.73,0.001,,,,,,60,110.01,3,167.6,0.007,60,53,40,7,,,,,,,,25,110,3.8,236.37,0.009364155,,,,,,,,,,,,,,,,,,,,,,,
25,109.8,2.6,81.79,0.015,25,38,45,18,,,,,,,,,,,,,,,,,,25,110.15,2.8,61.02,0.011,25,45,41,13,,,,,,,,,60,110,3.2,119.31,0.004,,,,,,40,109.95,3.1,66.52,0.002,,,,,,90,110,3,258.47,0.011,90,45,45,10,,,,,,,,35,110,3.4,366.68,0.014526583,,,,,,,,,,,,,,,,,,,,,,,
35,110.04,2.4,116.6,0.021,35,26,50,24,,,,,,,,,,,,,,,,,,35,110.07,2.9,90.77,0.016,35,34,46,20,,,,,,,,,180,110,3.1,500,0.022,,,,,,60,110,3.2,86.64,0.003,,,,,,120,110,2.9,353.02,0.016,120,32,51,17,,,,,,,,45,110,3,401.36,0.015900483,,,,,,,,,,,,,,,,,,,,,,,
45,109.99,2.4,136.72,0.025,45,24,46,30,,,,,,,,,,,,,,,,,,45,110.03,2.8,120,0.022,45,29,46,25,,,,,,,,,300,110,3,856.65,0.037,,,,,,90,110,3.1,82.4,0.003,,,,,,180,110,2.9,537.06,0.024,180,22,53,25,,,,,,,,56,110,2.6,620.84,0.024595515,,,,,,,,,,,,,,,,,,,,,,,
60,109.99,2.5,204.67,0.037,60,12,46,42,,,,,,,,,,,,,,,,,,60,110.01,2.8,160.43,0.029,60,21,45,34,,,,,,,,,,,,,,,,,,,120,110,3.1,207.74,0.01,,,,,,240,110,2.8,703.63,0.031,240,14,51,35,,,,,,,,80,110,2.6,873.58,0.034608193,,,,,,,,,,,,,,,,,,,,,,,
80,110,2.4,242.06,0.044,80,10,39,51,,,,,,,,,,,,,,,,,,80,109.97,2.8,203.6,0.037,80,14,43,43,,,,,,,,,,,,,,,,,,,180,110,3.1,348.7,0.016,,,,,,300,110,2.9,848.53,0.037,360,9,41,50,,,,,,,,110,110,2.6,1114.8,0.044164488,,,,,,,,,,,,,,,,,,,,,,,
130,110,2.2,319.39,0.058,130,0,31,69,,,,,,,,,,,,,,,,,,100,110.01,2.8,234.12,0.043,100,8,40,51,,,,,,,,,,,,,,,,,,,240,110,3,480.9,0.021,,,,,,360,110,2.9,998.96,0.043,426,4,40,56,,,,,,,,140,110,2.5,1289.71,0.051093812,,,,,,,,,,,,,,,,,,,,,,,
160,110.01,2.2,350.95,0.063,160,0,23,77,,,,,,,,,,,,,,,,,,130,109.95,2.7,276.44,0.05,130,6,31,62,,,,,,,,,,,,,,,,,,,300,110,2.9,604.48,0.026,,,,,,426,110,2.9,1119.05,0.048,486,3,37,60,,,,,,,,170,110,2.4,1442.46,0.057145234,,,,,,,,,,,,,,,,,,,,,,,
190,109.97,2.1,376.56,0.068,190,0,19,81,,,,,,,,,,,,,,,,,,160,110,2.7,304.79,0.055,160,5,28,67,,,,,,,,,,,,,,,,,,,360,110,3,670.36,0.029,,,,,,486,110,2.9,1220.41,0.053,540,3,34,63,,,,,,,,230,110,2.4,1691.88,0.067026385,,,,,,,,,,,,,,,,,,,,,,,
240,109.99,2,397.92,0.072,240,0,14,86,,,,,,,,,,,,,,,,,,190,110.01,2.7,332.76,0.06,190,0,25,75,,,,,,,,,,,,,,,,,,,600,110.02,3,996.62,0.043,,,,,,540,110,2.9,1283.86,0.055,600,3,29,68,,,,,,,,,,,,0,,,,,,,,,,,,,,,,,,,,,,,
300,110.01,2,420.47,0.076,300,0,9,91,,,,,,,,,,,,,,,,,,240,110,2.7,356.38,0.064,240,0,20,80,,,,,,,,,,,,,,,,,,,780,110,3,1275.97,0.055,,,,,,600,110,2.9,1358.96,0.059,798,0,22,78,,,,,,,,,,,,0,,,,,,,,,,,,,,,,,,,,,,,
360,110.06,2.2,430.74,0.078,360,0,8,92,,,,,,,,,,,,,,,,,,300,109.99,2.8,394.42,0.071,300,0,15,85,,,,,,,,,,,,,,,,,,,1308,110,3.1,1590.17,0.069,,,,,,798,110,2.9,1618.84,0.07,1392,0,10,90,,,,,,,,,,,,0,,,,,,,,,,,,,,,,,,,,,,,
420,108.73,2,442.33,0.08,420,0,4,96,,,,,,,,,,,,,,,,,,360,110.01,2.8,399.92,0.072,360,0,10,90,,,,,,,,,,,,,,,,,,,1368,110,3,1597.13,0.069,,,,,,1392,110,2.9,1937.4,0.084,1440,0,4,96,,,,,,,,,,,,0,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,420,110,2.8,412.82,0.075,420,0,8,92,,,,,,,,,,,,,,,,,,,,,,,,,,,,,1440,110,2.9,1903,0.083,,,,,,,,,,, ,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,480,109.95,2.7,425.78,0.077,480,0,8,92,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
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,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,25242,,,,,,,,,,,,
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Experiment FL 4a,54.25°C at t = 0,min = °C,Ret time 5.113,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,Experiment FL 13b,54.25°C at t = 0,min = °C,Ret time 5.113,PLA grade 2500HP,,NMR,NMR,NMR,,,,,,,,,Experiment FL 32a,50.02°C at t = 0,min = 48.74°C,Ret time 5.104,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,Experiment FL 32b,50.02°C at t = 0,min = 48.66°C,Ret time 5.041,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,Experiment FL 32e,50.02°C at t = 0,min = 48.52°C,Ret time 5.02,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,Experiment FL 32f,50.12°C at t = 0,min = 48.88°C,Ret time 5.02,PLA grade 6202D,,NMR,NMR,NMR
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of eythl lactate ,Time (m),INT (PLA),CE (Oligomer),Et-La
0,54.25,0.7,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,0,54.25,1.5,0,0,0,100,0,0,,,,,,,,,0,50.02,0.4,0,0,0,100,0,0,,,,,,,,,0,50.02,0.3,0,0,0,100,0,0,,,,,,,,,0,50.02,0.2,0,0,0,100,0,0,,,,,,,,,,,,,0,50.12,0.4,,0,0,100,0,0
30,50.71,0.6,0,0,30,92,8,0,,,,,,,,,,,,,,,,,,60,50,1.4,2.83,0.001,60,85,14,1,,,,,,,,,10,50.95,0.4,115.87,0.004,10,0,9,91,,,,,,,,,10,50.5,0.3,16.89,0.000669123,10,50,24,26,,,,,,,,,10,50.92,0.2,107.94,0.0043,10,35,27,38,,,,,,,,,,,,,10,50.81,0.4,21.35,0.000845813,10,57,20,23
60,49.99,0.6,1.58,0.001,60,92,8,0,,,,,,,,,,,,,,,,,,120,50,4.4,6.66,0.002,120,78,20,1,,,,,,,,,30,50.05,0.4,303.54,0.014,30,0,7,93,,,,,,,,,30,50,0.3,167.8,0.006647651,30,32,28,40,,,,,,,,,30,50.05,0,356.3,0.0141,30,16,28,56,,,,,,,,,,,,,20,50.05,0,,0,20,37,27,36
120,50,0.6,3.32,0.001,120,84,15,1,,,,,,,,,,,,,,,,,,300,50,6.5,19.89,0.004,300,64,30,6,,,,,,,,,60,50.01,0.4,478.56,0.022,60,0,9,91,,,,,,,,,60,50,0.3,313.4,0.012415815,60,20,29,51,,,,,,,,,60,50,0,663.68,0.0263,60,8,24,68,,,,,,,,,,,,,30,50,0,175.61,0.006957056,30,30,28,42
180,50,1,10.02,0.002,180,80,18,2,,,,,,,,,,,,,,,,,,810,50,5.8,92.62,0.017,810,32,44,24,,,,,,,,,90,50,0.4,591.61,0.026,90,0,7,93,,,,,,,,,90,50,0.3,428.84,0.016989145,90,13,29,58,,,,,,,,,90,50,0,869.96,0.0345,90,5,19,76,,,,,,,,,,,,,45,50,0,282.29,0.011183345,45,20,30,50
360,50,1,21.57,0.004,360,68,27,6,,,,,,,,,,,,,,,,,,1530,50,6.1,173.05,0.031,1530,22,39,39,,,,,,,,,120,50,0.4,698.37,0.031,120,0,10,90,,,,,,,,,120,50,0.3,521.66,0.02066635,120,10,28,62,,,,,,,,,120,50,0,1058.81,0.0419,120,4,16,80,,,,,,,,,,,,,60,50,0,379.54,0.015036051,60,15,29,56
600,50,0.8,43.06,0.007,600,55,36,8,,,,,,,,,,,,,,,,,,2430,50,5.7,242.39,0.044,2430,10,30,60,,,,,,,,,180,50,0.4,867.91,0.038,180,0,16,84,,,,,,,,,180,50,0.3,649.42,0.025727755,180,7,26,67,,,,,,,,,150,50,0,1200.53,0.0476,150,4,11,85,,,,,,,,,,,,,90,50,0,511.29,0.020255527,90,10,27,63
1080,50,0.7,99.65,0.018,1080,33,43,23,,,,,,,,,,,,,,,,,,3690,50,5.4,332.88,0.06,3690,3,21,75,,,,,,,,,240,50.02,0.4,1029.48,0.044,240,4,15,81,,,,,,,,,240,50,0.3,775.96,0.030740829,240,5,24,71,,,,,,,,,180,50,0,1330.11,0.0527,180,1,14,85,,,,,,,,,,,,,120,50,0,619.95,0.024560257,120,7,26,67
1620,50,0.7,156.75,0.028,1620,21,43,36,,,,,,,,,,,,,,,,,,4320,50,9.3,322.42,0.058,4320,0,13,87,,,,,,,,,318,50,0.4,1167.1,0.051,316,3,21,76,,,,,,,,,300,50,0.3,851.86,0.033747722,300,4,23,73,,,,,,,,,210,50,0,1406.59,0.0557,210,1,11,88,,,,,,,,,,,,,180,50,0,779.95,0.030898899,180,4,24,72
2550,50,0.7,239.85,0.043,2550,8,36,56,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,360,50,0.4,1206.91,0.052,360,5,20,75,,,,,,,,,360,50,0.3,891.04,0.035299897,360,4,21,75,,,,,,,,,240,50,0,1492.21,0.0591,240,1,10,89,,,,,,,,,,,,,240,50,0,911.7,0.036118374,240,3,21,76
3270,50,0.9,293.18,0.053,3270,1,23,76,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,420,50,0.4,1312.1,0.057,420,6,21,74,,,,,,,,,420,50,0.3,975.94,0.038663339,420,3,20,77,,,,,,,,,300,50,0,1590.64,0.063,300,0,7,93,,,,,,,,,,,,,300,50,0,999.32,0.039589573,300,1,20,79
4650,50,1,355.05,0.064,4650,0,19,81,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,618,50,0.4,1418.64,0.062,618,5,20,75,,,,,,,,,948,50,0.3,1333.44,0.052826242,948,1,15,84,,,,,,,,,1110,50,0,2076.99,0.0823,1110,0,2,98,,,,,,,,,,,,,420,50,0,1136.18,0.045011489,420,2,15,83
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,672,50,0.4,1430.53,0.062,672,5,21,74,,,,,,,,,1350,50,0.3,1396.7,0.055332383,1350,1,13,86,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,1314,50,0,1611.64,0.063847556,1314,3,1,96
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,1290,50,0.5,1739.67,0.075,1290,4,14,82,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,0,100,0,0,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,1350,50,0.4,1707.32,0.075,1350,4,15,81,,,,,,,,,,,,0,0,,,,,,,,,,,,,,,,,,10,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,16.89,0.001,,,,,,,,,,,,,,,,,,30,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,167.8,0.007,,,,,,,,,,,,,,,,,,60,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,313.4,0.012,,,,,,,,,,,,,,,,,,90,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,428.84,0.017,,,,,,,,,,,,,,,,,,120,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,521.66,0.021,,,,,,,,,,,,,,,,,,150,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,649.42,0.026,,,,,,,,,,,,,,,,,,180,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,775.96,0.031,,,,,,,,,,,,,,,,,,210,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,851.86,0.034,,,,,,,,,,,,,,,,,,240,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,891.04,0.035,,,,,,,,,,,,,,,,,,300,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,975.94,0.039,,,,,,,,,,,,,,,,,,1110,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,1333.44,0.053,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,1396.7,0.055,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,