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Experiment E6a,130.44°C at t = 0,min = 127.86°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,Experiment E7a,121.3°C at t = 0,min = 119.18°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,Experiment E8a,108.59°C at t = 0,min = 105.34°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La
0,130.44,5.7,0,0,,,,,,,,,,,0,121.3,4.3,0,0,,,,,,,,,0,108.59,3.2,0,0,,,,
10,132.27,5.7,12.76,0.000505367,,,,,,,,,,,20,120.86,4.3,159.25,0.00630718,,,,,,,,,25,110.12,3.2,48.82,0.001933542,,,,
20,137.26,5.6,137.26,0.005436255,,,,,,,,,,,40,119.98,4.3,480.32,0.019023328,,,,,,,,,60,109.97,3.3,275.79,0.010922809,,,,
40,130.06,5.5,305.31,0.012091964,,,,,,,,,,,60,199.97,4.2,680.67,0.026958295,,,,,,,,,90,109.99,3.3,427.56,0.01693374,,,,
60,130,5.5,481.06,0.019052636,,,,,,,,,,,90,119.65,4.3,874.44,0.034632659,,,,,,,,,140,109.99,3.3,644.79,0.025537249,,,,
90,130.08,5.5,778.77,0.030843598,,,,,,,,,,,150,119.98,4.3,1238.77,0.049062141,,,,,,,,,210,109.99,3.3,882.09,0.034935641,,,,
120,129.96,5.6,979.28,0.038784902,,,,,,,,,,,210,120,4.4,1573.98,0.06233831,,,,,,,,,300,110.03,3.4,1088.97,0.043129233,,,,
180,130,5.8,1282.81,0.050806369,,,,,,,,,,,240,120,4.4,1633.59,0.064699196,,,,,,,,,420,110,3.3,1284.42,0.050870133,,,,
240,130,5.8,1319.89,0.052274942,,,,,,,,,,,RAN ON METHANOL METHOD,,,,,,,,,,,,,,,,,,,,,
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Experiment E6b,130.38°C at t = 0,min = 128.67°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,Experiment E7b,122.16°C at t = 0,min = 119.74°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,,,,,,,,,
0,130.38,5.5,0,0,,,,,,,,,,,0,122.16,4.3,0,0,,,,,,,,,,,,,,,,,
15,130.93,5.5,54.61,0.002162858,,,,,,,,,,,20,120.75,4.3,162.45,0.006433918,,,,,,,,,,,,,,,,,
30,130.13,5.5,287.11,0.011371143,,,,,,,,,,,40,120,4.3,484.15,0.019175017,,,,,,,,,,,,,,,,,
60,130.01,5.6,554.77,0.021971959,,,,,,,,,,,60,120.01,4.3,695.28,0.027536932,,,,,,,,,,,,,,,,,
90,129.9,5.5,875.96,0.034692859,,,,,,,,,,,90,120,4.3,788.69,0.031236485,,,,,,,,,,,,,,,,,
150,129.99,5.5,1151.03,0.045587152,,,,,,,,,,,120,119.99,4.3,1138.62,0.045095647,,,,,,,,,,,,,,,,,
210,130,5.5,1488.39,0.058948473,,,,,,,,,,,180,119.96,4.4,1443.92,0.057187215,,,,,,,,,,,,,,,,,
300,130,5.5,1657.93,0.065663195,,,,,,,,,,,240,119.99,4.4,1651.64,0.065414076,,,,,,,,,,,,,,,,,
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Experiment E6c,130°C at t = 0,min = 121.92°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,,,,,,,,,,,,,,,,,,,,,,,,
0,130,5.5,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
20,130.32,5.5,33.47,0.001325597,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
40,129.97,5.5,282.97,0.011207177,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
60,130.01,5.6,498.02,0.019724346,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
90,129.97,5.6,788.39,0.031224603,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
120,129.97,5.6,1071.21,0.042425839,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
180,129.98,5.6,1388.82,0.055004951,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
240,129.98,5.6,1740.16,0.068919957,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
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Experiment E6d,130.34°C at t = 0,min = 127.97°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,,,,,,,,,,,,,,,,,,,,,,,,
0,130.34,5.5,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,
30,130.22,5.5,104,0.004118975,30,48,18,34,,,,,,,,,,,,,,,,,,,,,,,,,,,,
60,129.96,5.3,781.3,0.0309438,60,7,19,74,,,,,,,,,,,,,,,,,,,,,,,,,,,,
90,129.92,5.4,1114.7,0.044148283,90,0,12,88,,,,,,,,,,,,,,,,,,,,,,,,,,,,
120,130.01,54,1367.12,0.054145511,120,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
180,129.92,5.3,1656.61,0.065610915,180,0,7,93,,,,,,,,,,,,,,,,,,,,,,,,,,,,
240,130,5.3,1795.82,0.071124401,240,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
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Experiment E6e,130.96°C at t = 0,min = 128.55°C,Ret time 4.929,PLA grade 6202D,,NMR,NMR,NMR,,,,,,,,,,,,,,,,,,,,,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of ethyl lactate ,Time (m),INT (PLA),CE (Oligomer),Me-La,,,,,,,,,,,,,,,,,,,,,,,,,,,,
0,130.96,5.5,0,0,0,100,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,
20,130.81,5.5,84.81,0.003358945,20,48,19,33,,,,,,,,,,,,,,,,,,,,,,,,,,,,
40,130.04,5.5,544.05,0.021547388,40,14,23,63,,,,,,,,,,,,,,,,,,,,,,,,,,,,
60,129.97,5.5,747.87,0.029619787,60,4,27,69,,,,,,,,,,,,,,,,,,,,,,,,,,,,
90,129.93,5.5,1130.48,0.044773258,90,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
120,129.99,5.6,1358.15,0.053790249,120,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
180,130.04,5.6,1668.39,0.066077468,180,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
240,129.96,5.6,,0,240,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,