ZnAc 1 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,ZnAc 1 mol% 300rpm,,,17699,Max 0.0289 gml-1 ,,,DMAP 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,ZnAc 1 mol% DMAP 0.5 mol% TBD 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
Experiment P1a,130.82°C at t = 0,min = 125.21°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,Experiment P1c,130.87°C at t = 0,min = 129.55°C,Ret time 4.395,PLA grade 6202D,,,Experiment P10a,130.34°C at t = 0,min = 128.42°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,Experiment P16a,128.84°C at t = 0,min = 128.34°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Experiment P27a,125.32°C at t = 0,min = 119.29°C,Ret time 4.395,PLA grade 6202D,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
0,130.82,6.9,0,0,0,,,,,,,,,,,,0,130.87,5.7,0,0,0,,0,130.34,7,0,0,0,,,,,,,,,,,,,,,0,128.84,6.7,0,0,0,,,,,,,,,,,,,,,,,,,0,125.32,7.8,0,0,0
10,131.16,6.9,11.89,0.000671789,1.16226534,,,,,,,,,,,,30,130.38,5.7,64.69,0.003655009,12.64708913,,30,130.46,7,18.55,0.000904922,1.565609328,,,,,,,,,,,,,,,10,125.68,6.7,27.96,0.001363969,2.359807914,,,,,,,,,,,,,,,,,,,20,131.72,8,439.16,0.021423484,37.06485134
20,130.92,6.9,81.46,0.00460252,7.962837226,,,,,,,,,,,,60,129.98,5.6,117.24,0.006624103,22.92077182,,60,130.074,6.9,86.82,0.004235329,7.32755805,,,,,,,,,,,,,,,20,129.11,7.9,167.31,0.008161862,14.12086774,,,,,,,,,,,,,,,,,,,40,130.01,7.8,1058.57,0.05164008,89.34269897
60,129.99,6.8,268.3,0.015159049,26.22672757,,,,,,,,,,,,90,130,5.6,138.84,0.007844511,27.14363664,,120,129.95,6.9,303.52,0.014806576,25.61691337,,,,,,,,,,,,,,,30,129.75,8.2,487.46,0.023779697,41.14134355,,,,,,,,,,,,,,,,,,,60,130,8,1231.15,0.060059027,103.9083517
120,130.02,6.9,488.27,0.027587434,47.72912512,,,,,,,,,,,,150,130,5.5,160.87,0.009089214,31.45056775,,210,130.04,7,663.24,0.032354749,55.97707442,,,,,,,,,,,,,,,40,135.46,9.5,754.6,0.036811552,63.68780585,,,,,,,,,,,,,,,,,,,90,129.99,8,1277.55,0.062322552,107.824485
180,130,6.9,654.08,0.03695576,63.93730141,,,,,,,,,,,,,,,,,,,300,130,7,949.42,0.04631543,80.13050177,,,,,,,,,,,,,,,52,131.03,8.6,1044.02,0.050930289,88.11468734,,,,,,,,,,,,,,,,,,,,,,,,
240,130,6.9,669.19,0.037809481,65.41432658,,,,,,,,,,,,ZnAc 1 mol% 300rpm,Fresh catalyst ,,17699,Max 0.0289 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,ZnAc 1 mol% DMAP 0.5 mol% TBD 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
,,,,,,,,,,,,,,,,,Experiment P1d,131.17°C at t = 0,min = 130.3°C,Ret time 4.395,PLA grade 6202D,,,DMAP 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,Experiment P27b,127.48°C at t = 0,min = 125.68°C,Ret time 4.395,PLA grade 6202D,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,Experiment P10b,131.7°C at t = 0,min = 128.14°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,Experiment P16b,130.38°C at t = 0,min = 128.34°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
ZnAc 1 mol% 300rpm,,,17699,,,,,,,,,,,,,,0,131.17,5.6,0,0,0,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,0,127.48,7.8,0,0,0
Experiment P1b,130.18°C at t = 0,min = 122.47°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,30,130.4,5.6,99.41,0.005616702,19.43495332,,0,131.7,7,0,0,0,,,,,,,,,,,,,,,0,130.38,7.9,0,0,0,,,,,,,,,,,,,,,,,,,20,131.04,7.9,342.93,0.016729109,28.9430947
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,60,130.01,5.5,164.81,0.009311826,32.22084957,,30,130.23,6.9,4.48,0.000218547,0.378109423,,,,,,,,,,,,,,,15,131.96,7.9,421.27,0.020550759,35.55494563,,,,,,,,,,,,,,,,,,,40,130.06,8,1017.13,0.049618518,85.84518681
0,130.18,6.5,0,0,0,,,,,,,,,,,,120,130,5.5,226.04,0.012771343,44.19149832,,60,130,6.9,43.74,0.002133763,3.691630835,,,,,,,,,,,,,,,30,130.42,7.8,1037.06,0.050590761,87.52726734,,,,,,,,,,,,,,,,,,,60,130.06,8.2,1096.05,0.053468462,92.50598941
15,128.02,6.5,8.603,0.000486073,0.840956158,,,,,,,,,,,,180,130,5.5,253.74,0.014336403,49.60693144,,120,130,6.9,136.43,0.006655447,11.51461351,,,,,,,,,,,,,,,45,129.95,8.1,1108.91,0.05409581,93.59136601,,,,,,,,,,,,,,,,,,,90,130.01,8.6,1182.79,0.057699888,99.8267955
30,129.74,6.9,60.39,0.003412057,5.903213111,,,,,,,,,,,,,,,,,,,210,130.05,7,347.19,0.016936924,29.30263625,,,,,,,,,,,,,,,60,129.95,8.3,1205.09,0.058787746,101.7089027,,,,,,,,,,,,,,,,,,,,,,,,
60,130,7,197.87,0.011179728,19.34208939,,,,,,,,,,,,ZnAc 4 mol% 300rpm,,,17699,Max 0.0289 gml-1 ,,,360,130,7,758.66,0.03700961,64.03046752,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,MgAc 1 mol% DMAP 0.5 mol% TBD 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
120,130,7,525.28,0.029678513,51.34690815,,,,,,,,,,,,Experiment P4a,131.05°C at t = 0,min = 129.96°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,Experiment P28a,125.33°C at t = 0,min = 122.61°C,Ret time 4.395,PLA grade 6202D,
180,130.06,7,501.2,0.028317984,48.99305202,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,DMAP 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,Experiment P16c,129.58°C at t = 0,min = 127.57°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
,,,,,,,,,,,,,,,,,0,131.05,5.6,0,0,0,,Experiment P10c,130.43°C at t = 0,min = 128.14°C,Ret time 4.395,PLA grade 6202D,,,,,,MgAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,0,125.33,7.8,0,0,0
ZnAc 2 mol% 300rpm,,,17699,,,,,,,,,,,,,,30,130.35,5.6,155.98,0.008812927,30.49455808,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,Experiment P13b,130.71°C at t = 0,min = 126.73°C,Ret time 4.395,PLA grade 6202D,,,,,,0,129.58,7.4,0,0,0,,,,,,,,,,,,,,,,,,,20,131.36,7.9,159.1,0.007761354,13.42794846
Experiment P2a,130.40°C at t = 0,min = 127.55°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,60,130.01,5.6,234.08,0.013225606,45.76334244,,0,130.43,6.9,0,0,0,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,15,130.61,7.4,138.29,0.006746183,11.67159644,,,,,,,,,,,,,,,,,,,40,130.02,7.9,882.89,0.043069906,74.51540804
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,90,130,5.6,249.59,0.014101927,48.79559399,,60,130.06,6.9,25.48,0.001242987,2.15049734,,,,,0,130.71,7.8,0,0,0,,,,,30,130.27,7.6,828.6,0.040421484,69.93336328,,,,,,,,,,,,,,,,,,,60,129.98,8.2,1037.56,0.050615152,87.56946706
0,130.4,6.6,0,0,0,,,,,,,,,,,,120,129.96,5.6,266.65,0.015065823,52.13087518,,120,130.05,7,182.42,0.008898971,15.39614305,,,,,20,131.15,7.8,124.27,0.006062247,10.4883165,,,,,45,129.91,7.8,1150.49,0.056124201,97.10069408,,,,,,,,,,,,,,,,,,,90,129.98,8.4,1139.21,0.05557393,96.14866857
30,130.39,6.6,350.7,0.019814679,34.2814512,,,,,,,,,,,,,,,,,,,210,130,7.2,414.38,0.020214645,34.97343359,,,,,40,130.03,7.8,785.99,0.038342846,66.33710379,,,,,60,129.99,8.1,1272.63,0.062082541,107.4092398,,,,,,,,,,,,,,,,,,,,,,,,
60,130,6.6,684.91,0.038697667,66.95098016,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,17699,Max 0.0289 gml-1 ,,,300,130,7.2,685.87,0.033458705,57.8870334,,,,,60,129.94,8,1032.73,0.050379531,87.16181784,,,,,,,,,,,,,,,,,,,,,,,,,,,,,MgAc 1 mol% DMAP 0.5 mol% TBD 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
90,130.02,6.7,741.7,0.041906322,72.50228787,,,,,,,,,,,,Experiment P2d,131.05°C at t = 0,min = 129.96°C,Ret time 4.395,PLA grade 6202D,,,420,130,7.2,978.51,0.047734524,82.58568103,,,,,80,130,8.2,1156.91,0.056437387,97.64253839,,,,,ZnAc 2 mol% 600rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,Experiment P28b,126.77°C at t = 0,min = 121.52°C,Ret time 4.395,PLA grade 6202D,
150,129.96,6.7,951.25,0.053745974,92.98611479,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,100,130,8.3,1204.84,0.05877555,101.6878028,,,,,Experiment P16d,128.04°C at t = 0,min = 127.59°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
180,130,6.7,855.96,0.048362054,83.67137431,,,,,,,,,,,,0,131.05,5.5,0,0,0,,DMAP 2 mol% 300rpm,,,20499,Max 0.0482 gml-1 ,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,0,126.77,7.6,0,0,0
,,,,,,,,,,,,,,,,,30,130,5.5,133.51,0.007543364,26.10160565,,Experiment P11a,130..82°C at t = 0,min = 127.7°C,Ret time 4.395,PLA grade 6202D,60ml not 50ml,,,,,MgAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,0,129.58,8,0,0,0,,,,,,,,,,,,,,,,,,,30,130.17,7.6,214.99,0.010487829,18.14503231
ZnAc 2 mol% 300rpm,,,17699,,,,,,,,,,,,,,60,130.02,5.5,193.3,0.010921521,37.79073007,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,Experiment P13c,130.65°C at t = 0,min = 126.64°C,Ret time 4.395,PLA grade 6202D,,,,,,15,131.1,8,193.01,0.009415581,16.28993295,,,,,,,,,,,,,,,,,,,60,129.9,7.7,1192.99,0.058197473,100.6876696
Experiment P2b,130.28°C at t = 0,min = 126.42°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,90,130.02,5.5,242.1,0.013678739,47.33127651,,0,130.82,7.3,0,0,0,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,30,130.09,8.1,1032.53,0.050369774,87.14493795,,,,,,,,,,,,,,,,,,,90,130.06,7.9,1271.39,0.06202205,107.3045845
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,120,130.01,5.5,258.86,0.014625685,50.60790681,,30,130.4,7.3,5.83,0.000284404,0.590050036,,,,,0,130.65,7.8,0,0,0,,,,,45,130.06,8.3,1135.12,0.055374409,95.80347493,,,,,,,,,,,,,,,,,,,120,130,8.1,1281.11,0.062496219,108.1249469
0,130.28,6.7,0,0,0,,,,,,,,,,,,,,,,,,,60,130.02,7.2,51.64,0.002519147,5.22644663,,,,,20,131.35,7.8,147.92,0.007215962,12.4843629,,,,,60,129.91,8.5,1209.74,0.059014586,102.10136,,,,,,,,,,,,,,,,,,,,,,,,
30,130.18,6.7,78.68,0.004445449,7.691088054,,,,,,,,,,,,,,,,,,,120,130.05,7.4,187.83,0.009162886,19.01013692,,,,,40,129.98,7.4,577.48,0.02817113,48.73897976,,,,,,,,,,,,,,,,,,,,,,,,,,,,,TBD 1 mol% MgAc 0.5 mol% ZnAc 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
60,129.97,6.7,424.72,0.023996836,41.51701727,,,,,,,,,,,,,,,,,,,210,129.98,7.5,471.88,0.023019659,47.75862966,,,,,60,129.7,7.4,1116.24,0.054453388,94.21001379,,,,,ZnAc 1 mol% TBD 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,Experiment P29a,121.28°C at t = 0,min = 121.52°C,Ret time 4.395,PLA grade 6202D,
90,130,6.8,592.82,0.033494548,57.94904449,,,,,,,,,,,,P1 select average,,,,,,,300,130.2,7.5,677.76,0.033063076,68.59559387,,,,,80,129.99,7.8,1142.06,0.055712962,96.38920693,,,,,Experiment P17a,127.01°C at t = 0,min = 127.23°C,Ret time 4.395,PLA grade 6202D,PUMP issues,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
120,130.02,7,710.72,0.040155941,69.47394639,,,,,,,,,,,,Time,conversion ,,,,,,420,130.02,7.6,858.12,0.041861554,86.84969756,,,,,100,103,8,1207.76,0.058917996,101.9342491,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,0,121.28,7.6,0,0,0
180,130,7,997.88,0.056380586,97.54426726,,,,,,,,,,,,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,0,127.01,7.9,0,0,0,,,,,,,,,,,,,,,,,,,20,129.97,7.6,17.17,0.000837602,1.449138122
,,,,,,,,,,,,,,,,,30,20.16515703,,,,,,DMAP 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,TBD 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,15,130.86,7.9,335.81,0.016381775,28.3421708,,,,,,,,,,,,,,,,,,,40,129.94,7.8,491.33,0.023968486,41.46796932
ZnAc 3 mol% 300rpm,,,17699,,,,,,,,,,,,,,60,48.03459856,,,,,,Experiment P11b,130.64°C at t = 0,min = 125.86°C,Ret time 4.395,PLA grade 6202D,,,,,,Experiment P14a,130.55°C at t = 0,min = 127.98°C,Ret time 4.395,PLA grade 6202D,,,,,,30,130.07,8,786.12,0.038349188,66.34807572,,,,,,,,,,,,,,,,,,,60,129.9,8,782.15,0.03815552,66.01301
Experiment P3a,131.63°C at t = 0,min = 127.27°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,90,69.90112045,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,Int,CE,AL,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,45,129.98,8.3,1042.4,0.050851261,87.97796027,,,,,,,,,,,,,,,,,,,90,129.9,8.1,1059.74,0.051697156,89.4414463
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,120,67.82096852,,,,,,0,130.64,7.7,0,0,0,,,,,0,130.55,6.5,0,0,0,,,,,60,129.95,8.5,1120.87,0.054679253,94.60078313,, MgAc 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,MgAc 1 mol% TBD 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,120,129.99,8.2,1139.78,0.055601737,96.19677625
0,131.63,6.6,0,0,0,,,,,,,,,,,,75,46.30048694,,,,,,60,130.063,7.7,50.51,0.002464023,4.26301494,,,,,60,129.99,6.5,575.86,0.028092102,48.60225269,,,,,,,,,,,,Experiment P19a,130°C at t = 0,min = 124.74°C,Ret time 4.395,PLA grade 6202D,,,,,,Experiment P23a,128.04°C at t = 0,min = 119.24°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
20,130,6.6,216.68,0.0122425,21.18079511,,,,,,,,,,,,,,,,,,,120,130,7.7,358.21,0.017474511,30.23271791,16,52,32,,120,129.99,6.6,972.62,0.047447193,82.08856842,,,,,ZnAc 1 mol% TBD 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,TBD 1 mol% MgAc 0.5 mol% ZnAc 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
40,130.03,6.6,556.94,0.031467315,54.44172065,,,,,,,,,,,,,,,,,,,180,129.96,8,731.96,0.035707108,61.77700288,,,,,180,129.95,6.6,1081.63,0.052765013,91.2889497,,,,,Experiment P17b,130°C at t = 0,min = 125.3°C,Ret time 4.395,PLA grade 6202D,,,0,130,7.7,0,0,0,,,,,0,128.04,7.8,0,0,0,,Experiment P29b,126.56°C at t = 0,min = 125.88°C,Ret time 4.395,PLA grade 6202D,
60,130.01,6.6,674.13,0.038088593,65.89721899,,,,,,,,,,,,P2 select average,,,,,,,240,130.02,8.1,949.36,0.046312503,80.1254378,,24,76,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,30,130.13,7.7,432.58,0.021102493,36.50950312,,,,,15,131.89,8.1,55.05,0.002685497,4.646188328,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
90,130,6.8,777.39,0.04392282,75.99103892,,,,,,,,,,,,Time,conversion ,,,,,,300,130,8.2,1127.03,0.054979755,95.12068358,,11,89,,TBD 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,0,127.01,7.9,0,0,0,,60,129.97,8,1162.07,0.056689107,98.07803942,,,,,30,130.37,8.1,965.84,0.047116445,81.51634032,,0,126.56,7.6,0,0,0
120,130.01,6.8,854.95,0.048304989,83.5726453,,,,,,,,,,,,0,0,,,,,,,,,,,,,,,,Experiment P14b,130.85°C at t = 0,min = 127.82°C,Ret time 4.395,PLA grade 6202D,,,,,,15,131.71,7.9,251.99,0.012292795,21.26781102,,90,129.96,8.2,1272.83,0.062092297,107.4261197,,,,,45,130.11,8.3,1196.72,0.058379433,101.0024795,,30,130.22,7.6,137.94,0.006729109,11.64205664
160,130,6.8,930.48,0.052572462,90.95581613,,,,,,,,,,,,30,37.07421157,,,,,,DMAP 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,30,130.2,7.8,1007.57,0.049152154,85.03832831,,,,,,,,,,,,60,129.97,8.4,1260.1,0.061471291,106.351715,,60,129.92,7.7,935.61,0.045641739,78.96494571
,,,,,,,,,,,,,,,,,60,68.3375852,,,,,,Experiment P11c,130.47°C at t = 0,min = 124.59°C,Ret time 4.395,PLA grade 6202D,,,,,,0,130.85,6.5,0,0,0,,,,,45,130,8,1222.81,0.059652178,103.2044605,, MgAc 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,80,130.01,8.8,1269.24,0.061917167,107.1231258,,90,130.07,7.7,988.07,0.048200888,83.39253953
ZnAc 3 mol% 300rpm,,,17699,,,,,,,,,,,,,,90,76.95926754,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,Int,CE,AL,,30,130.34,6.5,429.76,0.020964925,36.27149674,,,,,60,130,8.3,1241.02,0.060540514,104.741374,,Experiment P19b,126.16°C at t = 0,min = 121.91°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,120,129.84,7.8,1029.29,0.050211718,86.87148381
Experiment P3b,131.18°C at t = 0,min = 127.13°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,135,92.67722005,,,,,,0,130.47,7.8,0,0,0,100,0,0,,60,130,6.5,798.53,0.038954583,67.39547258,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,MgAc 1 mol% TBD 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,165,90.50176041,,,,,,60,130.02,7.8,89.59,0.004370457,7.561344456,54,37,9,,90,130.05,6.7,955.79,0.046626177,80.6681261,,,,,ZnAc 1 mol% TBD 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,0,126.16,7.8,0,0,0,,,,,Experiment P23b,125.53°C at t = 0,min = 125.43°C,Ret time 4.395,PLA grade 6202D,,,DMAP 1 mol% MgAc 0.5 mol% ZnAc 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
0,131.18,6.7,0,0,0,,,,,,,,,,,,,,,,,,,120,130.01,7.7,495.78,0.02418557,41.84354676,8,52,40,,120,130,6.7,1039.52,0.050710766,87.73488993,,,,,Experiment P17c,130.21°C at t = 0,min = 125.25°C,Ret time 4.395,PLA grade 6202D,,,20,130.49,7.8,403.12,0.01966535,34.02309607,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,Experiment P30a,124.88°C at t = 0,min = 121.34°C,Ret time 4.395,PLA grade 6202D,
30,130.4,6.7,272.3,0.01538505,26.61773357,,,,,,,,,,,,P3 select average,,,,,,,180,129.97,7.8,791,0.038587248,66.75994491,0,39,60,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,40,129.87,7.8,1166.48,0.056904239,98.45024088,,,,,0,125.53,7.8,0,0,0,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
60,129.97,6.6,600.7,0.033939771,58.71932631,,,,,,,,,,,,Time,conversion ,,,,,,240,130.05,8.1,1033.5,0.050417094,87.22680539,0,22,78,,TBD 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,0,130.21,7.9,0,0,0,,60,129.95,8,1275.74,0.062234255,107.671722,,,,,15,131.34,7.8,25.34,0.001236158,2.138681421,,0,124.88,7.6,0,0,0
90,130,6.7,759.82,0.042930109,74.27354506,,,,,,,,,,,,0,0,,,,,,300,129.97,8.2,1147.29,0.055968096,96.83061593,0,13,87,,Experiment P14c,130.66°C at t = 0,min = 127.62°C,Ret time 4.395,PLA grade 6202D,8ml instead of 10ml MeOH,,,,,15,131.48,8,264.08,0.01288258,22.28820007,,80,130,8.3,1307.65,0.063790917,110.3649077,,,,,30,130.06,8,750.31,0.036602273,63.32573232,,30,130.22,7.6,438.54,0.021393239,37.01252369
120,129.99,6.9,811.49,0.045849483,79.32436509,,,,,,,,,,,,25,33.64802148,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,30,130.27,8,1074.45,0.052414752,90.68296183,,,,,,,,,,,,45,130.03,8.3,1065.06,0.051956681,89.89045123,,60,130,7.8,1145.75,0.05589297,96.70064081
180,130.02,7,910.48,0.051442454,89.00078612,,,,,,,,,,,,50,64.98519749,,,,,,MgAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,0,130.66,6.6,0,0,0,,,,,45,130.05,8.3,1225.79,0.059797551,103.4559708,, MgAc 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,60,130,8.5,1168.09,0.05698278,98.58612396,,90,130,7.8,1189.47,0.058025757,100.3905837
,,,,,,,,,,,,,,,,,75,75.26474528,,,,,,Experiment P12a,130.37°C at t = 0,min = 127.91°C,Ret time 4.395,PLA grade 6202D,Cooler switched on at 21min,,,,,30,130.45,6.6,246.01,0.012001073,20.76310246,,,,,60,130.01,8.5,1232.21,0.060110737,103.9978151,,Experiment P19c,128.48°C at t = 0,min = 122.17°C,Ret time 4.395,PLA grade 6202D,,,,,,80,129.99,8.8,1183.56,0.057737451,99.89178306,,,,,,,
ZnAc 2 mol% 300rpm,,,17699,,,,,,,,,,,,,,105,86.91281407,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,60,129.97,6.6,653.17,0.031863506,55.12717221,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,DMAP 1 mol% MgAc 0.5 mol% ZnAc 0.5 mol%,600rpm ,,20499,Max 0.0578 gml-1 ,
Experiment P2c,130.74°C at t = 0,min = 127.91°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,126.5,89.55014955,,,,,,0,130.37,7,0,0,0,,,,,90,130,6.7,849.79,0.041455193,71.72178709,,,,, TBD 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,0,128.48,7.8,0,0,0,,,,,MgAc 1 mol% TBD 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,Experiment P30b,128.34°C at t = 0,min = 127.29°C,Ret time 4.395,PLA grade 6202D,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,30,130.37,7,22.26,0.001085907,1.878731193,,,,,120,129.98,6.9,925.91,0.045168545,78.14627129,,,,,Experiment P18a,129.39°C at t = 0,min = 128.45°C,Ret time 4.395,PLA grade 6202D,,,20,131.24,8.1,172.26,0.008403337,14.53864489,,,,,Experiment P23c,122.88°C at t = 0,min = 118.44°C,Ret time 4.395,PLA grade 6202D,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
0,130.74,6.6,0,0,0,,,,,,,,,,,,P4 select average,,,,,,,60,130,7,157.85,0.007700376,13.32244918,,,,,180,130.11,6.9,957.86,0.046727157,80.84283291,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,40,129.96,8.1,847.09,0.041323479,71.49390864,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,0,128.34,7.6,0,0,0
30,130.27,6.6,407.84,0.02304311,39.86697194,,,,,,,,,,,,Time,conversion ,,,,,,120,130,7,423.73,0.020670764,35.76256821,,,,,,,,,,,,,,,0,129.39,7.7,0,0,0,,60,129.92,8.4,1154.79,0.056333968,97.46361161,,,,,0,122.88,7.8,0,0,0,,20,130.73,7.6,210.26,0.010257086,17.74582303
60,129.98,6.6,713.28,0.040300582,69.72419023,,,,,,,,,,,,0,0,,,,,,180,130.12,7.1,661.36,0.032263037,55.8184035,,,,,TBD 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,30,130.06,7.7,362.19,0.017668667,30.56862762,,80,130.07,8.6,1258.43,0.061389824,106.210768,,,,,15,130.34,7.7,40.53,0.00197717,3.420708682,,40,129.98,7.5,821.75,0.040087321,69.35522722
90,130.06,6.6,832.89,0.047058591,81.4162472,,,,,,,,,,,,30,40.27997203,,,,,,240,130.01,7.2,859.05,0.041906922,72.50332576,,,,,Experiment P15a,129.59°C at t = 0,min = 123.59°C,Ret time 4.395,PLA grade 6202D,,,,,,60,130.03,7.9,1033.2,0.050402459,87.20148556,,,,,,,,,,,,30,130.2,7.9,1179.55,0.057541831,99.55334136,,60,130.05,7.8,1050.13,0.051228353,88.63036782
120,130,6.8,944.93,0.053388892,92.36832531,,,,,,,,,,,,60,70.91480351,,,,,,300,130.04,7.4,935.65,0.04564369,78.96832169,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,90,130,8.1,1284,0.062637202,108.3688613,, DMAP 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,45,129.92,8.1,1291.39,0.062997707,108.992573,,90,130,8,1192.66,0.058181375,100.6598178
150,130,6.8,995.71,0.056257981,97.3321465,,,,,,,,,,,,90,82.82240253,,,,,,,,,,,,,,,,0,129.59,7.6,0,0,0,,,,,120,130,8.4,1284.41,0.062657203,108.403465,,Experiment P20a,126.22°C at t = 0,min = 121.84°C,Ret time 4.395,PLA grade 6202D,,,,,,60,129.95,8.4,1317.86,0.06428899,111.2266258,,,,,,,
,,,,,,,,,,,,,,,,,120,90.90840665,,,,,,MgAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,20,130.6,7.6,97.64,0.004763159,8.240759824,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,80,129.95,8.7,1345.27,0.065626128,113.540014,,DMAP 0.5 mol% TBD 0.5 mol% MgAc 0.5 mol% ZnAc 0.5 mol% ,600rpm ,,20499,Max 0.0578 gml-1 ,
ZnAc 2 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,165,90.7192575,,,,,,Experiment P12b,130.47°C at t = 0,min = 127.51°C,Ret time 4.395,PLA grade 6202D,,,,,,40,130.27,7.7,450.45,0.021974243,38.01772084,,,,, TBD 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,0,126.22,7.8,0,0,0,,,,,,,,,,,,Experiment P31a,128.99°C at t = 0,min = 126.42°C,Ret time 4.395,PLA grade 6202D,
Experiment P2e,130.30°C at t = 0,min = 127.47°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,60,130.11,7.9,744.75,0.036331041,62.85647152,,,,,Experiment P18b,130.30°C at t = 0,min = 128.09°C,Ret time 4.395,PLA grade 6202D,,,60,130,7.8,24.03,0.001172252,2.028118175,,,,,MgAc 1 mol% DMAP 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,0,130.47,6.9,0,0,0,,,,,90,130.02,7.9,884.97,0.043171374,74.69095885,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,120,129.98,8.1,118.46,0.005778818,9.997955846,,,,,Experiment P24a,127.79°C at t = 0,min = 124.33°C,Ret time 4.395,PLA grade 6202D,,,0,128.99,7.6,0,0,0
0,130.3,6.7,0,0,0,,,,,,,,,,,,,,,,,,,60,130,6.9,48.5,0.002365969,4.093372096,,,,,120,129.94,8.1,1076.03,0.052491829,90.81631292,,,,,0,130.3,7.7,0,0,0,,180,130,8.4,277.93,0.013558222,23.4571321,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,20,130.97,7.9,130.35,0.006358847,11.00146501
30,130.42,6.7,243.05,0.013732414,23.75850218,,,,,,,,,,,,,,,,,,,120,129.98,7,226.79,0.011063467,19.14094552,,,,,150,129.86,8.3,1100.27,0.053674326,92.86215498,,,,,20,130.76,7.8,114.71,0.005595883,9.681458003,,,,,,,,,,,,0,127.79,7.8,0,0,0,,40,129.95,7.9,523.23,0.02552466,44.16031097
60,130.02,6.7,570.72,0.03224589,55.78873633,,,,,,,,,,,,,,,,,,,180,130.01,7.1,413.38,0.020165862,34.88903417,,,,,,,,,,,,,,,40,130.05,7.9,343.46,0.016754964,28.9878264,, DMAP 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,20,131.12,8,113.52,0.005537831,9.581022688,,60,129.94,7.9,977.26,0.047673545,82.48018175
90,130.03,6.8,626.2,0.03538053,61.21198957,,,,,,,,,,,,,,,,,,,270,130,7.2,668.91,0.032631348,56.45561915,,,,,TBD 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,60,129.92,8.2,570.4,0.027825748,48.14143183,,Experiment P20b,126.84°C at t = 0,min = 121.42°C,Ret time 4.395,PLA grade 6202D,,,,,,40,130,7.9,723.55,0.035296844,61.06720372,,90,129.98,8.4,1210.28,0.059040929,102.1469357
120,130,6.9,777.62,0.043935816,76.01352177,,,,,,,,,,,,,,,,,,,360,130,7.2,884.13,0.043130397,74.62006333,,,,,Experiment P15b,130.63°C at t = 0,min = 125.68°C,Ret time 4.395,PLA grade 6202D,,,,,,90,130.03,8.6,776.95,0.037901849,65.57413299,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,60,129.97,8.1,981.81,0.047895507,82.86419913,,120,129.98,8.4,1248.27,0.06089419,105.3532698
180,130.2,7.3,953.47,0.053871405,93.20312312,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,120,130,8.9,913.49,0.044562662,77.09803044,,0,126.22,7.8,0,0,0,,,,,90,130.01,8.3,1101.31,0.05372506,92.94993038,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,MgAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,0,130.63,7.4,0,0,0,,,,,,,,,,,,60,130.02,7.9,14.68,0.000716132,1.238983554,,,,,,,,,,,,DMAP 0.5 mol% TBD 0.5 mol% MgAc 0.5 mol% ZnAc 0.5 mol% ,600rpm ,,20499,Max 0.0578 gml-1 ,
ZnAc 4mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,Experiment P12c,130.33°C at t = 0,min = 127.43°C,Ret time 4.395,PLA grade 6202D,,,,,,30,130.45,7.4,311.98,0.015219279,26.33093251,,,,, TBD 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,120,129.92,8.2,85.61,0.004176301,7.225434746,,,,,MgAc 1 mol% DMAP 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,Experiment P31b,126.67°C at t = 0,min = 123.42°C,Ret time 4.395,PLA grade 6202D,
Experiment P4b,130.30°C at t = 0,min = 127.50°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,60,129.93,7.5,761.36,0.037141324,64.25834596,,,,,Experiment P18c,129.96°C at t = 0,min = 127.47°C,Ret time 4.395,PLA grade 6202D,,,180,129.97,8.5,190.95,0.009315089,16.11607014,,,,,Experiment P24b,127.44°C at t = 0,min = 124.36°C,Ret time 4.395,PLA grade 6202D,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,0,130.33,6.9,0,0,0,,,,,90,130,7.6,946.07,0.046152007,79.84776369,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,0,126.67,7.6,0,0,0
0,130.3,6.6,0,0,0,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,17699,Max 0.0578 gml-1 ,,,60,130,6.9,49.15,0.002397678,4.148231722,,,,,120,130.02,7.8,1141.69,0.055694912,96.35797915,,,,,0,129.96,7.7,0,0,0,, DMAP 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,0,127.44,7.8,0,0,0,,30,130.12,7.5,427.52,0.020855651,36.08244203
30,130.41,6.6,369.71,0.020888751,36.13970723,,,,,,,,,,,,Experiment P5a,130.10°C at t = 0,min = 127.89°C,Ret time 4.395,PLA grade 6202D,,,120,130.03,6.9,203.1,0.0099078,17.14152315,,,,,150,129.97,7.9,1067.34,0.052067906,90.08288192,,,,,30,130.1,7.7,252.69,0.012326943,21.32689062,,Experiment P20c,128.26°C at t = 0,min = 126.5°C,Ret time 4.395,PLA grade 6202D,,,,,,30,129.8,7.5,515.04,0.025125128,43.46907968,,60,129.95,7.8,1219.38,0.059484853,102.9149704
60,130,6.6,730.22,0.041257698,71.38010065,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,180,130,7,379.47,0.018511635,32.02704968,,,,,,,,,,,,,,,60,130,7.9,700.65,0.034179716,59.13445689,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,60,130.04,7.7,1196.25,0.058356505,100.9628118,,90,129.99,8.1,1328.05,0.064786087,112.0866559
90,130.01,6.6,866.9,0.048980168,84.74077573,,,,,,,,,,,,0,130.1,7,0,0,0,,300,129.95,7.2,696.69,0.033986536,58.80023517,,,,,TBD 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,90,129.97,8.1,959.69,0.04681643,80.99728386,,0,128.26,7.8,0,0,0,,,,,90,129.9,8,1335.59,0.06515391,112.7230276,,120,130,8.3,1318.14,0.064302649,111.2502576
120,130.02,6.7,960.15,0.054248828,93.85610314,,,,,,,,,,,,30,130.13,7,375.25,0.021201763,36.68125054,,420,129.98,7.3,940.5,0.045880287,79.3776589,,,,,Experiment P15c,129.48°C at t = 0,min = 122.29°C,Ret time 4.395,PLA grade 6202D,,,,,,120,130,8.6,1082.05,0.052785502,91.32439746,,60,129.92,7.8,4.79,0.00023367,0.404273244,,,,,120,130.06,8.4,1334.66,0.065108542,112.6445361,,,,,,,
150,130,6.9,965.11,0.054529069,94.34095059,,,,,,,,,,,,60,129.96,7.2,778.27,0.043972541,76.07706024,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,150,130,8.9,1175.89,0.057363286,99.24443947,,120,129.95,8.1,29.15,0.001422021,2.460243229,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,90,130.01,7.4,911.01,0.0514724,89.05259441,,MgAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,0,129.48,7.6,0,0,0,,,,,,,,,,,,,,,,,,,,,,MgAc 1 mol% DMAP 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,
ZnAc 4mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,120,130,7.4,969.12,0.054755636,94.7329341,,Experiment P13a,130.37°C at t = 0,min = 126.27°C,Ret time 4.395,PLA grade 6202D,,,,,,30,130.12,7.6,200.19,0.009765842,16.89592082,,,,, TBD 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,ZnAc 1 mol% DMAP 1 mol%,600rpm 130C,,20499,Max 0.0578 gml-1 ,,,,,,Experiment P24c,127.83°C at t = 0,min = 123.88°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
Experiment P4c,130.50°C at t = 0,min = 128.58°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,60,130.19,7.6,743.67,0.036278355,62.76532014,,,,,Experiment P18d,122.96°C at t = 0,min = 117.54°C,Ret time 4.395,PLA grade 6202D,,,Experiment P21a,128.85°C at t = 0,min = 123.89°C,Ret time 4.395,PLA grade 6202D,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,17699,Max 0.0578 gml-1 ,,,0,130.37,7.4,0,0,0,,,,,90,129.95,7.8,1036.43,0.050560027,87.47409571,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,0,127.83,7.8,0,0,0,,,,,,,
0,130.5,6.7,0,0,0,,,,,,,,,,,,Experiment P5b,128.38°C at t = 0,min = 126.74°C,Ret time 4.395,PLA grade 6202D,,,30,130.66,7.4,232.7,0.011351773,19.63974612,,,,,120,129.94,8,1112.99,0.054294844,93.93571566,,,,,0,122.96,7.7,0,0,0,,0,128.85,7.8,0,0,0,,,,,30,130.01,7.8,381.56,0.018613591,32.20344448,,,,,,,
30,130.35,6.7,454.42,0.025674897,44.42023683,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,60,129.95,7.3,764.57,0.037297917,64.52926812,,,,,,,,,,,,,,,30,130.67,7.8,169.67,0.008276989,14.32005038,,20,130.31,7.9,336.96,0.016437875,28.43923014,,,,,60,130.07,8,1067.14,0.052058149,90.06600204,,,,,,,
60,129.96,6.6,720.7,0.040719815,70.44950636,,,,,,,,,,,,0,128.38,7.1,0,0,0,,120,130,7.4,1046.26,0.051039563,88.30374205,,,,,ZnAc 1 mol% DMAP 1 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,60,130,8,667.21,0.032548417,56.31214013,,40,130.02,8.1,1087.06,0.053029904,91.74723858,,,,,90,130,8.1,1186.92,0.057901361,100.1753651,,,,,,,
90,130.03,6.7,827.65,0.046762529,80.90402934,,,,,,,,,,,,30,129.35,7.1,73.83,0.004171422,7.216993277,,,,,,,,,,,,Experiment P32a,129.8°C at t = 0,min = 121.18°C,Ret time 4.395,PLA grade 6202D,,,,,,90,129.96,8.3,937.53,0.045735402,79.12699261,,60,129.95,8,1205.02,0.058784331,101.7029947,,,,,120,130.07,8.6,1265.93,0.061755695,106.8437637,,,,,,,
120,130.02,6.7,899.84,0.05084129,87.96071015,,,,,,,,,,,,60,129.97,7.1,553.95,0.031298378,54.14944367,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,120,130,8.5,1088.94,0.053121616,91.9059095,,80,130.03,8.3,1219.63,0.059497049,102.9360703,,,,,,,,,,,,,,,,,
180,129.8,7,891.01,0.050342392,87.0975644,,,,,,,,,,,,90,130.07,7.3,769.15,0.043457257,75.18556656,,,,,,,,,,,,0,129.8,7.6,0,0,0,,,,,150,130.05,9,1191.97,0.058147715,100.6015822,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,
,,,,,,,,,,,,,,,,,120,130,7.4,911.19,0.05148257,89.07018968,,,,,,,,,,,,20,131.7,7.5,352.34,0.017188156,29.73729329,,,,,,,,,,,,ZnAc 1 mol% DMAP 1 mol%,600rpm 130C,,20499,Max 0.0578 gml-1 ,,,,,,Experiment P16e,126.6°C at t = 0,min = 122.73°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
ZnAc 3 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,40,131.38,7.6,1219.67,0.059499,102.9394463,,,,,,,,,,,,Experiment P21b,131.45°C at t = 0,min = 126.45°C,Ret time 4.395,PLA grade 6202D,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,
Experiment P3c,130.4°C at t = 0,min = 127.38°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,ZnAc 2 mol% 600rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,60,129.97,7.6,1294.13,0.063131372,109.2238274,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,0,126.6,7.8,0,0,0,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,Experiment P5c,130.06°C at t = 0,min = 129.44°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,0,131.45,7.8,0,0,0,,,,,20,130.58,7.8,241.95,0.011803015,20.4204408,,,,,,,
0,130.4,6.7,0,0,0,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,ZnAc 1 mol% DMAP 1 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,15,131.26,8.1,154.81,0.007552076,13.06587493,,,,,40,130,8,901.14,0.043960193,76.05569754,,,,,,,
30,130.96,6.7,471.76,0.026654613,46.11524785,,,,,,,,,,,,0,129.6,7.1,0,0,0,,,,,,,,,,,,Experiment P32b,130.3°C at t = 0,min = 122.26°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,30,130.05,8.1,878.25,0.042843553,74.12379471,,,,,60,129.98,8.1,1060.18,0.05171862,89.47858204,,,,,,,
60,129.97,6.7,772.66,0.043655574,75.52867433,,,,,,,,,,,,30,130.05,7.1,422.79,0.02388779,41.32835687,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,45,130,8.5,1083.52,0.052857213,91.44846461,,,,,90,130,8.5,1159.79,0.056577882,97.88560873,,,,,,,
90,129.95,6.9,865.79,0.048917453,84.63227156,,,,,,,,,,,,60,130.1,7.2,773.77,0.043718289,75.63717849,,,,,,,,,,,,0,130.3,7.6,0,0,0,,,,,,,,,,,,60,129.94,8.7,1225.72,0.059794136,103.4500628,,,,,120,130,8.7,1186.07,0.057859896,100.1036256,,,,,,,
120,130.14,7,1000.85,0.056548393,97.83458921,,,,,,,,,,,,90,130.06,7.5,930.41,0.052568507,90.94897352,,,,,,,,,,,,15,131.78,7.7,336,0.016391043,28.35820669,,,,,,,,,,,,80,129.89,9.2,1271.13,0.062009366,107.2826407,,,,,,,,,,,,,,,,,
133,130.1,7,977.25,0.055214984,95.5276538,,,,,,,,,,,,120,130.08,7.7,1004.07,0.056730324,98.14934904,,,,,,,,,,,,30,130.77,7.8,1281.01,0.062491341,108.116507,,,,,,,,,,,,,,,,,,,,,,TBD 1 mol% DMAP 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,45,130.02,7.8,1396.65,0.068132592,117.8764565,,,,,,,,,,,,ZnAc 0.8 mol% DMAP 1.5 mol%,600rpm 130C (0.5g each),,20499,Max 0.0578 gml-1 ,,,,,,Experiment P25a,127.13°C at t = 0,min = 122.36°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
ZnAc 1 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,60,130.15,8.3,1424.09,0.069471194,120.1923767,,,,,,,,,,,,Experiment P22a,128.82°C at t = 0,min = 124.72°C,Ret time 4.395,PLA grade 6202D,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,
Experiment P1e,130.4°C at t = 0,min = 128.58°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,ZnAc 2 mol% 0rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,Int,CE,AL,,0,127.13,7.8,0,0,0,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,Experiment P6a,130.92°C at t = 0,min = 127.02°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,0,128.82,7.8,0,0,0,100,0,0,,30,130.27,7.9,112.63,0.005494414,9.5059072,,,,,,,
0,130.4,6.7,0,0,0,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,15,131.85,8,192.71,0.009400946,16.26461313,36,40,24,,60,129.98,8.4,512.75,0.025013415,43.275805,,,,,,,
30,130.3,6.7,253.96,0.014348833,24.82497105,,,,,,,,,,,,0,130.92,6.3,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,30,130.15,8,972.39,0.047435972,82.06915655,0,30,70,,90,129.94,8.4,742.25,0.036209083,62.64547296,,,,,,,
60,129.95,6.8,629.71,0.035578846,61.55509734,,,,,,,,,,,,30,130.12,6.3,128.72,0.007272727,12.58257314,,,,,,,,,,,,,,,,,,,,,,,,,,,,,45,129.83,8.2,1132.16,0.055230011,95.55365263,0,16,84,,120,129.99,8.7,928.22,0.045281233,78.34123396,,,,,,,
90,30.04,6.8,867.58,0.049018589,84.80724675,,,,,,,,,,,,60,130,6.3,420.01,0.023730719,41.0566077,,,,,,,,,,,,,,,,,,,,,,,,,,,,,60,129.91,8.5,1275.57,0.062225962,107.6573741,0,6,94,,180,130,9.3,1166.52,0.056906191,98.45361686,,,,,,,
120,130.05,6.8,813.73,0.045976044,79.54332845,,,,,,,,,,,,90,130,6.2,527.31,0.029793209,51.5453437,,,,,,,,,,,,,,,,,,,,,,,,,,,,,80,129.91,8.7,1334.39,0.065095371,112.6217483,0,2,98,,,,,,,,,,,,,,
150,130,6.8,947.31,0.053523363,92.60097388,,,,,,,,,,,,150,130,6.2,667.82,0.037732075,65.28040702,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,TBD 1 mol% DMAP 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,
,,,,,,,,,,,,,,,,,240,130.02,6.3,760.25,0.042954404,74.31557821,,,,,,,,,,,,,,,,,,,,,,,,,,,,,ZnAc 0.8 mol% DMAP 1.5 mol%,600rpm 130C (0.5g each),,20499,Max 0.0578 gml-1 ,,,,,,Experiment P25b,127.91°C at t = 0,min = 124.18°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
ZnAc 1 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,360,129.93,6.5,1037.61,0.058625346,101.4279344,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Experiment P22b,128.35°C at t = 0,min = 123.37°C,Ret time 4.395,PLA grade 6202D,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,
Experiment P1f,130.36°C at t = 0,min = 127.85°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,0,127.91,7.8,0,0,0,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,ZnAc 2 mol% 0rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,0,128.35,7.8,0,0,0,,,,,30,130.16,7.8,98.36,0.004798283,8.30152741,,,,,,,
0,130.36,6.8,0,0,0,,,,,,,,,,,,Experiment P6b,130.78°C at t = 0,min = 127.89°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,15,131.98,8.1,285.17,0.01391141,24.06818393,,,,,60,130.01,8,464.32,0.022650861,39.18834086,,,,,,,
30,130.46,6.8,158.62,0.008962088,15.505343,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,30,130.25,8,1104.62,0.053886531,93.22929247,,,,,90,129.98,8.1,666.73,0.032525001,56.27162841,,,,,,,
60,130.07,6.8,353.08,0.01994915,34.51409977,,,,,,,,,,,,0,130.78,6.3,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,45,129.99,8.1,1149.29,0.056065662,96.99941477,,,,,120,129.92,8.7,844.15,0.041180058,71.24577433,,,,,,,
90,130,6.9,562.6,0.031787107,54.99499415,,,,,,,,,,,,60,130,6.3,167.17,0.009445166,16.34111833,,,,,,,,,,,,,,,,,,,,,,,,,,,,,60,129.92,8.3,1281.61,0.062520611,108.1671466,,,,,180,122.31,7.7,1008.03,0.049174594,85.07715205,,,,,,,
120,129.47,7,573.89,0.032424996,56.09860859,,,,,,,,,,,,120,130.01,6.1,667.29,0.03770213,65.22859873,,,,,,,,,,,,,,,,,,,,,,,,,,,,,80,129.85,8.6,1316.09,0.064202644,111.0772388,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,180,129.97,6.1,839.61,0.047438273,82.07313728,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,ZnAc 1 mol% MgAc 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,
ZnAc 1 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,240,129.98,6.1,956.95,0.054068026,93.54329834,,,,,,,,,,,,,,,,,,,,,,,,,,,,, DMAP 2 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,Experiment P26a,126.72°C at t = 0,min = 124.83°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
Experiment P1g,129.94°C at t = 0,min = 126.35°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Experiment P20e,128.18°C at t = 0,min = 126.15°C,Ret time 4.395,PLA grade 6202D,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,
Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,ZnAc 2 mol% 0rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,0,126.72,7.8,0,0,0,,,,,,,
0,129.94,6.6,0,0,0,,,,,,,,,,,,Experiment P6c,130.81°C at t = 0,min = 128.02°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,0,128.18,7.8,0,0,0,,,,,30,130.26,7.7,448.76,0.0218918,37.87508581,,,,,,,
30,130.19,6.6,71.45,0.004036951,6.984344706,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,60,130.07,7.8,36.1,0.001761062,3.04681923,,,,,60,129.96,7.6,867.99,0.042343041,73.25785662,,,,,,,
60,130.02,6.4,574.9,0.032482061,56.1973376,,,,,,,,,,,,0,130.81,6.3,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,120,129.97,8,546.34,0.026652032,46.11078167,,,,,90,129.88,7.9,1057.1,0.051568369,89.21863181,,,,,,,
90,129.97,6.5,843.77,0.047673315,82.47978352,,,,,,,,,,,,60,129.98,6.3,155.02,0.008758687,15.1534376,,,,,,,,,,,,,,,,,,,,,,,,,,,,,180,130.06,9.4,903.75,0.044087516,76.27598004,,,,,120,129.99,8.1,1145.14,0.055863213,96.64915716,,,,,,,
120,130.01,6.6,822.8,0.046488502,80.42993456,,,,,,,,,,,,120,129.97,6.2,688.38,0.038893723,67.29017787,,,,,,,,,,,,,,,,,,,,,,,,,,,,,240,129.9,10.4,1110.65,0.054180692,93.73822101,,,,,,,,,,,,,,,,,
150,129.97,6.7,906.84,0.051236793,88.64497066,,,,,,,,,,,,180,130,6.2,779.23,0.044026781,76.17090169,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,ZnAc 1 mol% MgAc 1 mol%,600rpm,,20499,Max 0.0578 gml-1 ,,,,,,,,
,,,,,,,,,,,,,,,,,240,130,6.2,922.03,0.052095034,90.12981595,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Experiment P26b,125.18°C at t = 0,min = 123.13°C,Ret time 4.395,PLA grade 6202D,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,0,125.18,7.8,0,0,0,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P7a,130.62°C at t = 0,min = 129.47°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,30,130.06,7.6,340.58,0.016614469,28.74475605,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,60,129.94,7.8,926.91,0.045217328,78.23067072,,,,,,,
,,,,,,,,,,,,,,,,,0,130.62,6,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,90,130,8.2,1154.86,0.056337382,97.46951957,,,,,,,
,,,,,,,,,,,,,,,,,30,130.19,6,149.9,0.008469405,14.65294992,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,120,129.99,8.4,1152.66,0.05623006,97.28384084,,,,,,,
,,,,,,,,,,,,,,,,,60,130.04,6,244.09,0.013791175,23.86016374,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,90,129.97,6.1,292.95,0.016551783,28.63630205,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,150,130.02,6.2,330.35,0.018664896,32.29220817,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,210,130.03,6.4,391.27,0.022106899,38.24722958,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,17699,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P7b,130.85°C at t = 0,min = 129.86°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,130.85,6,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,60,130,6,156.84,0.008861518,15.33134533,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,120,129.99,6,321.64,0.018172778,31.4407926,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,180,130,6.1,383.37,0.021660546,37.47499272,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,300,129.85,6.1,502.17,0.028372789,49.08787097,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,420,130,6.2,589.46,0.033304706,57.62059945,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,18591,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P8a,130.39°C at t = 0,min = 125.13°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,130.39,7.1,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,30,130,7.1,595.23,0.032017105,55.39291531,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,60,130,7.1,1065.83,0.057330429,99.18759291,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,18591,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P8b,129.87°C at t = 0,min = 124.79°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,129.87,7.1,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,15,129.63,7.1,38.09,0.002048841,3.54470733,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,30,130.24,7.4,356.51,0.019176483,33.17730665,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,45,129.86,7.6,700.59,0.037684363,65.19786056,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,60,129.66,7.7,1044.52,0.056184175,97.20445526,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,18591,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P8c,131.72°C at t = 0,min = 125.32°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,131.72,7.4,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,20,131.85,7.4,491.54,0.026439675,45.74338255,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,40,130.12,7.3,965.66,0.051942338,89.86563614,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,50,130.05,7.4,1121.01,0.060298532,104.3227189,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,60,130.07,7.6,1145.61,0.061621752,106.6120285,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P9a,130.38°C at t = 0,min = 122.88°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,130.38,7.5,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,20,130.93,7.5,482.55,0.023540173,40.72694237,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,40,130.18,7.6,1205.15,0.058790673,101.7139666,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,50,129.95,7.9,1255.07,0.061225913,105.9271859,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,60,130,7.9,1227.7,0.059890726,103.6171737,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P9b,133.16°C at t = 0,min = 125.45°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,133.16,7.5,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,15,132.07,7.6,320.32,0.015626128,27.03482371,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,30,130.21,7.5,1198.91,0.058486268,101.1873142,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,40,130,7.6,1223.42,0.059681936,103.2559441,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P9c,131.06°C at t = 0,min = 123.56°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,131.06,7.5,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,15,131.35,7.5,449.35,0.021920581,37.92488147,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,30,130.67,7.7,1111.47,0.054220694,93.80742853,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,45,130,7.8,1192.57,0.058176984,100.6522219,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,ZnAc 2 mol% 300rpm,,,20499,Max 0.0578 gml-1 ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Experiment P9d,122.09°C at t = 0,min = 115.02°C,Ret time 4.395,PLA grade 6202D,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,Time (m),Temperture (°C),Pressure (bar),Peak area ,Concentration of MeLa,Conversion,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,0,122.09,5.8,0,0,0,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,15,123.04,7.3,72.84,0.003553344,6.147654093,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,30,130,7.5,625.93,0.03053466,52.82813188,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,45,129.76,7.5,917.16,0.044741695,77.40777633,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,60,130,7.8,1078.67,0.052620616,91.0391274,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,
,,,,,,,,,,,,,,,,,90,130,7.8,1245.61,0.060764428,105.1287674,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,