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    <data_prep_note>X-ray diffraction (XRD) data were collected using a Bruker D8 X-ray diffractometer with a linear position sensitive detector (PSD) (CuKα radiation). Room temperature XRD patterns were recorded over the 2θ range 15° to 80° with a 0.02° step size. For Rietveld refinement, data were collected over the 2θ range 15° to 120° with a 0.02° step size and structure refinement performed using the GSASII suite of Rietveld refinement software.</data_prep_note>
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